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铸造镍基高温合金K445的热疲劳行为

李友林 , 袁超 , 郭建亭

金属学报

利用开有V形缺口的平板试样,研究了一种新型铸造高温合金K445在最高温度分别为800、850、900℃,最低温度为室温的热循环下的热疲劳行为. 通过光学显微镜和扫描电镜观察合金的组织和热疲劳裂纹形貌,研究热疲劳损伤机制. 结果表明,热疲劳主裂纹主要从V形缺口处萌生,沿晶界扩展,而二次裂纹则穿晶扩展. 当最高循环温度为800℃时,碳化物的组成和分布起主要作用,(Ti, Ta)C的开裂处以及碳化物与基体分离的界面处是裂纹优先形成区域. 当最高循环温度为900℃时,高温氧化的作用占主导地位. 应力辅助作用下的晶界氧脆是此时的主要损伤机制.

关键词: 铸造高温合金 , thermal fatigue , carbide , oxidation

定向凝固DZ38G合金热疲劳性能和组织结构的研究

张静华 , 唐亚俊 , 于洋 , 张济山 , 胡壮麒

金属学报

本文研究了定向凝固DZ38G合金热疲劳性能及其组织结构的变化,并与其原型合金M38G对比.由于DZ38G合金消除了横向晶界和弹性模量低等原因,抗热疲劳性能有很大提高.热疲劳裂纹一般萌生在晶界或相界面,沿着枝晶间或晶界扩展,有时裂纹也沿着一定晶体学方向传播.合金经热疲劳后,晶界碳化物增多,γ′形态发生变化,并观察到裂纹两侧存在γ′相贫化和再结晶现象.

关键词: 定向凝固 , thermal fatigue , directional solidification , microstructure

3种铸造镍基高温合金热疲劳行为研究

肖旋许辉秦学智郭永安郭建亭周兰章

金属学报 doi:10.3724/SP.J.1037.2011.00066

研究了3种铸造镍基高温合金在不同温度下的热疲劳行为, 利用OM和SEM对合金的组织和热疲劳裂纹形貌进行了观察. 结果表明: 3种合金的热疲劳裂纹均萌生于V型缺口尖端处, 应力诱导下氧化孔洞的产生、聚集和相互连通是裂纹萌生的主要方式, 晶界、碳化物及共晶促进了裂纹的萌生和扩展. IN738和DZ444合金的热疲劳裂纹分别沿晶界和枝晶间扩展, DZ445合金的裂纹扩展方式随着温度升高由沿枝晶间扩展转变为沿晶体学取向扩展. 高温氧化和热应力的交互作用是热疲劳的主要损伤机制, 各合金在较高温度 (950℃) 下发生的微观组织演化促进了热疲劳性能的降低.

关键词: 镍基高温合金 , thermal fatigue , high-temperature oxidation , crystallographic orientation , microstructural evolution

INFLUENCE OF TOP TEMPERATURE OF THERMAL CYCLE ON THERMAL STRESS/STRAIN AND THERMAL FATIGUE BEHAVIOR OF PURE IRON

J.H.Liu 1) and S.H.Jiang 1) and M.Yao 2) 1) Department of mechanical Engineering , Engineering college , Yangzhou University , Yangzhou 225009 , China 2) Department of Material Science , Yanshan University , Qinhuangdao 066000 , China

金属学报(英文版)

By using a self-made thermal fatigue test machine of outer-constraint mode, the influence of top-temperature of thermal cycle T t on thermal stress-strain and thermal fatigue behavior of an industrial pure iron was investigated. The T t was varied from stress/strain 773K to 1073K. The results show that, increasing of T t , the thermal stress-strain cycles can be classified into four types, they are: compressive stress cycle; compressive strain-tensile stress cycle; compressive strain-tensile stress cycle than changing to compressive tensile plastic strain cycle; and finally, compressive tensile plastic strain cycle. It is also revealed that certain relationship does exist between thermal fatigue life and characteristics of thermal stress/strain cycle. When compressive tensile plastic strain cycle were appear by increasing of T t , thermal fatigue life decreasing rapidly. The concept of thermal fatigue transition temperature, and determining method were put up in this thesis.

关键词: thermal fatigue , null

灰铸铁的热疲劳特性及断裂力学计算分析

郭成璧 , 周玮生

金属学报

本文通过试验分析了灰铸铁的同相和异相热疲劳及C-P型和P-C型高温低周疲劳特性,并应用弹塑性断裂力学方法对其寿命作了解析评价。试验和计算都表明,在相同应变范围下,同相和C-P型疲劳寿命分别高于异相和P-C型。这与低碳钢等材料结果相反。另外,计算值和试验吻合,说明J积分用作评价灰铸铁热疲劳强度的力学参量及本文所建立的力学模型和计算方法有效。文中从能量角度提出了一个用于描述裂纹扩展能力的参量ΔW_T,在相同ΔW_T值下,高温低周疲劳寿命和热疲劳相等。

关键词: 灰铸铁 , thermal fatigue , fracture

交流电作用下Au薄膜热疲劳失效行为的研究

王鸣张滨刘常升张广平

金属学报 doi:10.3724/SP.J.1037.2010.00668

本文研究了交流电致循环热应变作用下200 nm厚Au薄膜的失效行为. 结合实验结果和理论计算, 确定了交流电作用下6 μm宽Au薄膜导线上的温度分布, 并由此确定了Au互连线在交流电作用下达到稳定状态后的循环热应变范围. 结果表明, 应变范围Δε≦0.35%, 经过5×106 cyc热循环后, Au互连线中的晶粒出现不同程度的增长, 晶界损伤导致Au互连线的最终失效. 对Au薄膜热疲劳、机械疲劳失效行为及其机制进行了分析.

关键词: Au薄膜 , alternating current , thermal fatigue

IN-SITU OBSERVATION OF THERMAL FATIGUE CRACK GROWTH IN STEEL 3Cr2W8V

LIU Jianhong HE Shiyu YAO Mei Harbin Institute of Technology , Harbin , China lecturer , Depatment of Metallic Materials , Harbin Institute of Technology , Harbin 150006 , China

金属学报(英文版)

The growing process of thermal fatigue cracking,in steel 3Cr2WSV was observed under desk SEM fitted with sell-made minisized device for thermal faligue test.Before the growing of thermal fatigue crack,the main crack tip reveals to blunt firstly,and some holes and uncontinuous microcraeks occur in front of it.The growth is developed by bridging of main crack together with holes and microcracks.

关键词: steel 3Cr2W8V , null , null , null

THERMAL FATIGUE AND FRACTURE MECHANICS ANALYSIS OF GREY CAST IRON

GUO Chengbi ZHOU Weisheng Dalian Institute of Technology , Dalian , Liaoning , China Professor , Dept.of Shipbuilding , Dalian Institute of Technology , Dalian , Liaoning , China

金属学报(英文版)

The in-phase and out-of-phase thermal fatigue,the C-P type and P-C type isothermal fa- tigue of grey cast iron were experimentally studied.The fatigue life was evaluated analytically by using the elastic-plastic fracture mechanics method(mainly J integral).The results of ex- periments and calculations showed that the lifes of in-phase and C-P type fatigue are longer than that of out-of-phase and P-C type fatigue respectively within the same strain range. This is in contrast to the results of other materials such as low carbon steel.On the other hand, the predicted lifes are consistent with experimental results.This suggests that J integral as a mechanics parameter for characterizing the thermal fatigue strength of grey cast iron and the mechanics model and the calculation method developed here are efficient.A parameter ΔW_1 was proposed from energy aspect to characterize the capacity of crack propagation. The isothermal fatigue life is the same as the thermal fatigue life for identical ΔW_1 values.

关键词: grey cast iron , null , null

国产1000MW超超临界机组水冷壁管典型横向裂纹分析

殷尊 , 蔡晖 , 侯召堂 , 张红军 , 刘鸿国

材料科学与工程学报

对国产1000MW超超临界燃煤机组水冷壁管普遍存在的横向裂纹进行分析研究,通过割取典型管样进行磁粉检测、显微组织分析、硬度试验、扫描电镜能谱分析、拉伸性能试验和断口分析,结果表明该锅炉水冷壁管表面横向裂纹是轴向交变应力作用下产生的热疲劳裂纹,腐蚀介质的存在加速了热疲劳裂纹的扩展.为防止此类失效问题,建议相关电厂采取了有效的针对性防范措施,同时对其它超超临界机组水冷壁管的安全运行提供技术参考.

关键词: 水冷壁管 , 横向裂纹 , 腐蚀介质 , 热疲劳 , 防范措施

灰口铸铁低频热疲劳载荷下的微观组织与拉伸性能

兰鹏 , 李阳 , 张家泉

材料热处理学报

实验分析了灰口铸铁经周期性的高温氧化处理后,其抗拉强度、基体组织、断口形貌与化学成分的变化规律,并探讨了热疲劳载荷下灰口铸铁失效的微观-宏观机制.结果表明:灰口铸铁的抗拉强度和抗热疲劳性能在微观上与石墨形貌、基体组织和晶粒尺寸有关,宏观上受温度、氧化条件、载荷周期和化学成分的影响.随着高温氧化处理次数增加,试样脱碳越来越明显,珠光体逐步减少直至消失;同时,短小而零碎的新石墨不断形成,断口处石墨暴露率逐步增大,基体连续性显著恶化;此外,试样基体铁素体化后,尽管脱碳速率降低,但基体晶粒逐步粗化、二次渗碳体析出使晶界弱化,各温度下抗拉强度随碳含量减小而显著下降.

关键词: 铸铁 , 热疲劳 , 微观组织 , 拉伸性能

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